Munzvimbo inoparadza zvakanyanya, online spectroscopy yekutarisa inova nzira inoshanda yekutsvagisa.
Lithium bis(fluorosulfonyl)amide (LiFSI) inogona kushandiswa seyekuwedzera yelithium-ion bhatiri electrolytes, ine zvakanakira senge yakakwira simba density, kugadzikana kwekupisa, uye kuchengetedzeka.Kudiwa kweramangwana kuri kuwedzera kuoneka, zvichiita kuti ive hotspot mune itsva simba indasitiri yekutsvaga zvinhu.
Iyo synthesis process yeLiFSI inosanganisira fluoridation.Dichlorosulfonyl amide inopindirana neHF, apo iyo Cl muchimiro chemolecular inotsiviwa naF, ichigadzira bis(fluorosulfonyl)amide.Munguva yekugadzira, zvigadzirwa zvepakati izvo zvisina kunyatsotsiviwa zvinogadzirwa.Mamiriro ekuita anoomesa: HF inoparadza zvakanyanya uye ine muchetura zvakanyanya;maitiro anoitika pasi pekushisa kwakanyanya uye kumanikidzwa, zvichiita kuti maitiro ave nengozi zvikuru.
Parizvino, kutsvagisa kwakawanda pamusoro pekuita uku kunotarisa pakutsvaga mamiriro ekuita kuti awedzere goho rechigadzirwa.Iyo yega nzira yekuona isina mhepo inowanikwa kune zvese zvikamu ndeye F nuclear magnetic resonance (NMR) spectrum.Nzira yekuona nayo yakaoma zvikuru, inotora nguva, uye ine ngozi.Munguva yese yekutsiva, iyo inogara kwemaawa akati wandei, kudzvanywa kunofanirwa kuburitswa uye samples dzinotorwa maminetsi ega ega 10-30.Aya masampuli anozoyedzwa neF NMR kuona zviri mukati mezvigadzirwa zvepakati uye zvigadzirwa.Kutenderera kwekusimudzira kwakareba, sampling yakaoma, uye sampling maitiro anokanganisa maitiro, zvichiita kuti data rebvunzo risamiririre.
Nekudaro, tekinoroji yekutarisa yepamhepo inogona kugadzirisa zvakakwana zvipimo zvekutarisa kunze kwenyika.Mukuita optimization, online spectroscopy inogona kushandiswa kutarisa chaiyo-nguva in-situ kutariswa kwezvinoita, zvigadzirwa zvepakati, uye zvigadzirwa.Iyo yekunyudza probe inosvika pazasi pemvura yemvura mu kettle yekupindura.Iyo probe inokwanisa kumira nekuora kubva kune zvinhu zvakaita seHF, hydrochloric acid, uye chlorosulfonic acid, uye inogona kushivirira kusvika ku200 ° C tembiricha uye 15 MPa kumanikidza.Girafu rekuruboshwe rinoratidza kutariswa kwepamhepo kwezvinoita uye zvigadzirwa zvepakati pasi pezvinomwe maitiro paramita.Pasi peparameta 7, izvo mbishi zvinopedzwa nekukurumidza, uye kuita kunopedzwa kwekutanga, zvichiita kuti ive yakanyanya kunaka maitiro.
Nguva yekutumira: Nov-23-2023